试题与答案

富马酸亚铁中砷盐的检查:取待测品0.50g,加入无水碳酸钠0.5g,混匀,加溴试液4

题型:单项选择题 共用题干题

题目:

富马酸亚铁中砷盐的检查:取待测品0.50g,加入无水碳酸钠0.5g,混匀,加溴试液4ml,置水浴上蒸干后,在500~600℃炽灼2小时,自然冷却,残渣加溴-盐酸溶液10ml与水15ml使溶解,移至蒸馏瓶中,加酸性氯化亚锡试液1ml,蒸馏,流出液导入贮有水5ml的接收器中,至蒸馏瓶中剩5ml时,停止蒸馏,馏出液加水适量使成28ml,按古蔡法检查砷盐。

提示加入含砷浓度为1μg/ml的标准砷溶液2ml。在该测定条件下,砷盐的限量是()

A.0.0002%

B.0.0004%

C.0.001%

D.0.002%

E.0.004%

F.0.005%

答案:

参考答案:B

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