试题与答案

(18分) 硫酸铜是一种应用极其广泛的化工原料.某课外兴趣小组将适量浓硝酸分多次

题型:实验题

题目:

(18分)

硫酸铜是一种应用极其广泛的化工原料.某课外兴趣小组将适量浓硝酸分多次加到铜粉与稀  硫酸的混合物中,加热使之反应完全(装置如题29图I、图Ⅱ所示),通过蒸发、结晶得到硫酸铜晶体,并同时测定硫酸铜晶体中结晶水的含量.

(1)怎样检查图I装置的气密性                                                

(2)图I中分液漏斗内装的液体是                               

(3)图Ⅱ是图Ⅰ的改进装置,与图I相比,图Ⅱ装置的明显优点是                     

                                                       ,(可不答满).

(4)课外兴趣小组同学在测定胆矾晶体中结晶水的含量时.测得有关数据如下表:

加热前质量加热后质量
m1(容器)m2(容器+晶体)m3(容器+无水CuSO4
5.4g7.9g6.8g
 

①为完成测定,题29图Ⅲ中还缺少的仪器名称是                            

②判断样品已恒重的方法是                                             

③测定所得胆矾中结晶水含量的实验中,称量操作至少进行     次。

④课外兴趣小组的测定结果x值(与相比        (填“偏高”、“偏低”、“不变”),可能的原因是                。(填字母序号)

a.加热温度过高                  b.胆矾晶体的颗粒较大

c.加热后放在空气中冷却          d.胆矾晶体部分风化

答案:

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参考答案:对

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